[COPY]

 

United States Patent [19]

H. E. Kistner, Sr.

 

[54]  FERTILIZER UTILIZING A

     CHlTIN-PRODUCING FUNGUS AND

     METHOD FOR ITS USE

 

 

[76]   Inventor:   Harold E. Kistner, Sr., 1500 W.

           Matlock, #22, Aransas Pass TX         ,

                   78336

[21]   Appl. No. : 764,932

[22]    Filed:     Aug. 12, 1985

[51]    Int, cl),4                       ....... CO5F 11/08;

[52]    U.S. CL                         .. .. .. 71/7;435/918;

                                         

[58]    Field of Search           ...... .. 426/331,634,807;

              47/57.6, DIG. 9, DIG. 10; 71/1, 6, 7; 435/171,

                                          915, 918; 424/115

 Patent Number:   4,670,037

 Date of Patent:   Jun. 2, 1987

 

             References Cited

[56]

       US. PATENT DOCUMENTS

    3,115,404 12/1963  Carney ....71/6

Primary examiner---Ferris H. Lander

                                                 

Attorney, Agent, or Firm-Pearne, Gordon, McCoy &

Granger

 

 

         [57] ABSTRACT A novel natural  fertilizer and method  of

         its use are Provided.  The  fertilizer acts to  increase

         the Yield of food crop producing plants.  The fertilizer

         comprises less than 0.05% of an active agent in a stable

         carrier that is non-toxic to the  plants and the  active

         agent.  The  active  agent  is a  fungus  of  the  genus

         Aspergillus.  The fertilizer can be used by coating  the

         seeds of the food  crop producing plant  at or prior  to

         the time of planting by dusting the ends of a cut plant,

         by dusting the roots of  a seedling, or by treating  the

         soil in which the plant will be grown.

 


 

         6   Claims,

 

         No   Drawings

         FERTILIZER  UTILIZING  A  CHITIN-PRODUCING  FUNGUS   AND

         METHOD FOR  ITS  USE BACKGROUND  OF  THE  INVENTION

 

         The invention relates  to fertilizers  and plant  growth

         and yield promoters,  and to  processes for  the use  of

         these products.

 

         Fertilizers and plant  growth and  yield promoters  have

         long been used to increase plant growth and crop  yield.

         While mankind first used natural products, such as waste

         products,  as  fertilizers,  the   use  of   synthesized

         fertilizers has become  increasingly  prevalent.    This

         proliferation of synthetic fertilizers has given rise to

         concern for  the health  of individuals  and  ecological

         systems exposed to these products and to the by-products

         from their production.

 

                                         

         The present  invention responds  to  these  concerns  by

         providing a  fertilizer having  an  active  agent  which

         occurs  naturally,   which   has   been   shown   causes

         significantcant  increases  in  plant  growth  and  crop

         yields,  and   which  is   relatively   economical   and

         convenient to use.  The active agent is a fungus of  the

         genus Aspergillus.

                                                         

         DISCUSSION  OF  THE  PREVIOUS  ART  Naturally  occurring

         products have long  been used as  fertilizers and  plant

         growth promoters.  Such products  have included  manure,

         fish products, and crop residues.

 

        

         Another example of naturally occurring products that are

         used in  agricultural science  are  certain  strains  of

         bacteria.  It   is  understood  that  the  addition   of

         bacteria such as Rhizobia and Azotobacter can aid plants

         in  the  breakdown  of  soil  materials  to  form  plant

         nutrients, as well as in the in fixation of  atmospheric

         nitrogen.  An example of a teaching illustrating this is

         found in US.   Pat.No.4,061,488 to  Mann, which  teaches

         methods of using a plant treating mixture  incorporating

         spores of Bacillus uniflagellatus.

 

      
                                      

         It has been  recognized as  well that  certain types  of

         fungus or  their products  can be  used by  agronomists.

         US.  Pat.   No.    4,370,351  relates  to  a  method  of

         producing a  food or  feed  product, such  as  a  cereal

         grain, which has been  treated with a  spawn culture  of

         Pleurotus to increase the protein  content of the  food.

 

 

         It is also known  that the  genus of fungi  used in  the

         present  invention,  Aspergillus,  can  be  useful   for

         agricultural purposes.  US.   Pat.    No.     3,043,748,

         having the  same  inventor  as  the  present  invention,

         discloses a product resulting  from the fermentation  of

         sucrose by Aspergillus us flavus, oryzae.  which  serves

         as a growth-promoting substance.

 

       OBJECTS AND SUMMARY OF THE

              INVENTION

        

         It is an object  Of the present  invention to provide  a

         new fertilizer or plant yield  and growth promoter  par-

         ticularly useful for commercial  plants such as  commer-

         cial crop producers.

 

 

         It is another object of the invention to provide methods

         for the use of the new fertilizer.

 

         The fertilizer of the present invention concerns the use

         of fungus as the active agent.  It is believed that  all

         chitin-producing fungi may  be used  in accordance  with

         the invention as a fertilizer.  However, the strains  of

         fungi which have been demonstrated to be useful are from

         the Euascomycetae subclass of  Asomycetes, and  carriers

         are finely ground calcium carbonate,  talc, and silt  or

         the material washed from sand.  An example of a material

         which has been found  to be unsuitable  as a carrier  is

         wheat middlings.  It is  believed  that  this  substance

         results in agglutination by the mold.

 

 

         The fertilizer should contain 5 to 500 parts per million

         parts (i.e., 0.0005%  to  0.05%) of  active  agent,  and

         preferably 5 to  100 parts per  million (i.e.,  0.0005%.

         to 0.01%), and most preferably 10 to 50 parts of  active

         agent per million (i.e., 0.001% to 0.005%).  Other plant

         growth additives   which  do  not  interfere  with   the

         intended tended activity  of  the active  agent  may  be

         added.  Trace  elements  would be  an  example  of  such

         additives.

 

 

         The fertilizer may be used in various  ways.  Seeds  may

         be coated at planting time or before planting time  with

         sufficient fertilizer to  coat  the  seed.    The  exact

         amount of  fertilizer necessary  to coat  the seed  will

         vary with the size  of  the seed.   Smaller  seeds  will

         require more, since  they have a  greater surface  area.

         One-half 20 cup of growth-promoter is sufficient to coat

         one bushel of seed corn.

 

         It is  also  possible to  dust  the cut  ends  of  plant

         cuttings before planting.  Plants that may be planted in

         this manner  ner  include  agricultural  crops  such  as

         potatoes, or even house  plants that are  grown in  this

         manner.

 

 

         The growth-promoter  may  be  dusted  on  the  roots  of

         seedlings which will be  transplanted, such as  tomatoes

         or cabbage.  The growth-promoter may  be applied, as  by

         dusting the tilled field, to the soil prior to planting.

         The following  examples demonstrate  the products,  use,

         and effectiveness of the growth-promoter of the  present

         invention.

 

PART 2 KISTNER CHITIN PATENT

 

                 EXAMPLE 1

 

         Production of the active agent for the fertilizer of the

         present invention can  be accomplished  as follows.    A

         culture  of  Aspergillus  flavus-oryzae,  NRRL  458,  is

         isolated by use of  Czapek-Dox medium with  agar.   This

         strain  of  fungi   is  on  deposit   at  the   Northern

         Utilization Branch  at  Peoria,  I11.    The  Czapek-Dox

         medium consists of NaNo3, 3.0 grams; K2HP04, 1 .0  gram;

         MgS04.7- H20, 0.5 gram; KC1, 0.5 gram; FeS04.7H20,  0.01

         gram; sucrose 30.0 grams; and agar 15.0 grams in 1 liter

         distilled water.  All components  are of reagent  grade.

         This medium is sterilized at 15  pounds pressure for  15

         minutes.  The medium  is inoculated with  spores of  the

         mold culture and is subsequently incubated at 25 degrees

         C.  for two  to three  days.   Single  colonies  of  the

         culture will develop velop and isolated mold spores  can

         be selected by a trained observer.

 

 

         The culture material that acts as  the active agent  can

         be prepared from the isolated mold  spores by either  of

         two  methods  The  culture  material  may  he  grown  in

         sterilized, distilled water that is aerated with air and

         carbon dioxide gas, or the culture material may be grown

         in any suitable carbohydrate medium, such as wheat  bran.

 

         To cause  growth  in water,  isolated  mold  spores  are

         introduced to sterilized, de ionized distilled water  in

         a flask by air floatation  of spores into the water  Air

         and carbon  dioxide are  bubbled through  the water  and

         mold mixture.  The mixture is incubated at 28 degrees C.

         until a sufficient quantity of  culture material  has

         grown.  The culture material is separated from the water

         by filtration, decanting or evaporation.   This is  used

         as the active agent.

 

         For the second growth method,  isolated mold spores  are

         air-floated into a  500 milliliter  flask containing  32

         grams of wheat  bran which  has been  moistened with  16

         milliliters of 0.   1 normal  hydrochloric  acid.    The

         inoculated bran is  incubated at  20"  to 25"  C.    The

         flasks should  be left  upright, until  rapid growth  is

         completed, specifically  when the  material will  remain

         caked in the bottom when  laid flat.   This material  is

         allowed to dry.   The  dried  material is  used  as  the

         active agent.  It  consists of fungus  and any  residual

         bran.

 

         In order to  assure  that the  proper amount  of  active

         agent  is  added   to  the  carrier   for  the   maximum

         efficiency, a sample  of  the active  agent  is  tested.

         This standardization  procedure can  be accomplished  by

         the fermentation of starch.   Fifty-six grams of  finely

         ground corn is placed in a 500 milliliter flask to which

         250 milliliters of  distilled  water  is  added.    This

         mixture is autoclaved at  15 pounds of  pressure for  15

         minutes.  The mixture is allowed to  cool to 61  degrees

         C.  and one gram of mold  spore culture is added to  the

         mixture.  This is cultured with yeast  at 28 degrees  C.

         This temperature is maintained  tained until the  growth

         medium is spent.  The weight loss  is measured every  12

         hours.

 

 

         In order to determine the glucose  which is produced  by

         the enzyme activity of the mold spore culture, a control

         is also  run  which  was not  treated  with  mold  spore

         culture.  The weight loss for the control represents the

         amount of fermentable sugar  native to the  corn.   This

         value is subtracted from the weight loss for the treated

         sample.  The  weight  of  the  carbon  dioxide  produced

         equals 95.5% of the value of the alcohol produced.   The

         weight of the  alcohol  produced equals  51.1 %  of  the

         value of the glucose fermented.  Thus, the weight of the

         carbon dioxide  produced equals  48.9%  of  the  glucose

         fermented.  It has been determined that  20 to 30  parts

         per million  of  active  agent in  the  carrier  is  the

         optimal  level   when  the   sample   which   has   been

         standardized results in the production of 12-14 grams of

         carbon dioxide over a 60-hour period.

 

               

 EXAMPLE 2

 

         This and the  following examples  illustrate methods  of

         using the invention, and demonstrate the efficacy of the

         present invention.    Active  agent  was  isolated   and

         prepared by  growth in  wheat bran  as described  above.

         The active agent was mixed, 25 parts per million  active

         agent in a  horizontal  mixer to  form  a  substantially

         uniform disbursement with a carrier  of fine silt  which

         was washed from alluvial deposit to form the  fertilizer

         of the present invention.  This carrier is also referred

         to as  sand  washings.    A  field  test  was  conducted

         comparing the crop yield and the root growth of  Lincoln

         pea plants  grown  from  treated  seeds  with  those  of

         Lincoln pea plants grown  from non-treated  seeds.   The

         seeds were treated  with the fertilizer  by coating  the

         seeds.  Two 13-foot  rows of treated  seed were  planted

         intermediate two 13-foot rows of untreated seed used  as

         a control.   Rows  I  and  IV  were  the  control  rows.


 

         Twenty-four inch netting  was placed over  the seeds  to

         protect the plants from pests.  The peas were allowed to

         mature and the  peas  were harvested  every  other  day,

         three times.  The yield is shown below.

 

                             Yield in Pounds

                              Control            Treated Seeds

                         Row I    Row IV      Row II   Row 111

First Harvest           0.90      1.40        1.30    1.70

Second Harvest       0.25      0.75        0.85     0.50

Third Harvest          0.00      0.10        0.00     0.20

                              1.15      2.25        2.15     2.40

 

         The total yield for the control  was 3.40 pounds,  while

         the total yield for the treated  seeds was 4.55  pounds.

         This represents  a  33.8%  increase  in  yield  for  the

         treated plants.  At the bloom stage and after harvest, a

         number of plants were carefully  removed from the  soil.

         The dirt was carefully  cleaned from the  roots so  that

         the root system and the nodules on the root system  were

         not disturbed.   The roots  were dried  and mounted  for

         com parison  of  the  root  system  and  the  nodules.

         Nodules are  round   swellings  on  a  root  which   are

         inhabited by symbiotic  bacteria.   These bacteria  help

         the plant to assimilate  needed nutrients, most  notably

         nitrogen.  Thus, an in- creased nodule count indicates a

         greater ability to as- similate nitrogen.  This in  turn

         contributes to greater crop  yield.   Comparison of  the

         roots of the treated  and the con-  trol plants both  at

         the bloom stage  and the  mature stage  shows a  greater

         root development and greater development of nodules in

         the treated plant.

 

                EXAMPLES 3-5

 

         Similar field tests were conducted  for red beets,  car-

         rots, and popcorn.  The tables below represent the  per-

         centage weight increase for the plants treated with  the

         fertilizer at  25 ppm  Aspergillus flavus-oryzae  active

         agent in  sand  washings as  compared  to  an  untreated

         control grown  at  the  same period  in  the  same  soil

         conditions in a neighboring plot.

 

                             Percentage Yield Increase

       Plant                     (by weight)

       Red beets                    50.0%

       Carrots                        37.5%

       Popcorn                      33.3%


 

 

         Comparative   photographs   of   the   resultant   crops

         illustrate that the individual  vegetables yielded  from

         the  treated  plants  were  generally  larger  than  the

         vegetables of the control plants.

 

              EXAMPLE 6

         A similar field test was conducted for Pontiac  potatoes

         The test crop was produced from  cuttings dusted at  the

         fresh  cut  end   with  a  fertilizer   having  25   ppm

         Aspergillus Flavus oryzae active agent in sand washings.

         A control crop  was  grown in  a neighboring  plot  from

         untreated cuttings.  The treated plants yielded 18.8% by

         weight more potatoes  than the  control  plants.    Once

         again,  comparative  photographs  illustrate  that   the

         treated  plants  yielded  a  generally  higher   quality

         product than the control plants.  .

 

              EXAMPLE 7

         A similar  field  test  was  conducted  for  Tendergreen

         beans.  The test crop was grown  from seeds coated  with

         25 ppm Aspergillus  flavus oryzae active  agent in  sand

         washings.  The control crop was grown at the same period

         in a neighboring  plot.    After  several  weeks,  young

         plants were removed  from the  ground and  the dirt  was

         carefully removed from the root system.  Care was  taken

         not to disturb root hairs and nodules on the roots.  The

         roots were carefully dried  and mounted far  comparison.

         A comparison between the estimated  num- ber of  visible

         nodules per plant on test plants and on treated   plants

         is seen below.

 

 

                   IMMATURE PLANTS

                                                          

       Plain        Nodule        Treated       Nodule

       Plants       Count         Plants        Count

                                                        

      Control 1     48-58        Test 1        56-66  

      Control 2      6-16         Test 2       18-28  

      Control 3     16-26        Test 3       36-46  

 

                                                       

         About four  weeks later,  mature plants  were  similarly

         removed from the ground.  The dirt was carefully removed

         from the root system.  The roots were dried and  mounted

         for comparison.  Because of more extensive root  system,

         it was difficult to estimate the  number of nodules  for

         the plants;  however, the  treated plant  ap- peared  to

         have significantly more nodules than the con- trol  and,

         further,  to  have   a  more   extensive  root   system.


 

 

EXAMPLE 8

                              

         A similar field  test was conducted  for Great  Northern

         Beans.  Test  plants were  grown from  seed dusted  with

         fertilizer of   the  invention  containing  25  ppm   of

         Aspergil-  lus  ,flavus  oryzae  active  agent  in  sand

         washings.  The control plants were grown from  untreated

         seed in a neighboring plot under the same conditions  as

         the test plants.   The  treated plants  yielded a  33.3%

         increase by weight in the yield.  After harvest,  plants

         were carefully removed from  the soil and  the dirt  was

         removed from the  root system  for a  comparison of  the

         roots of treated versus untreated plants, as in Examples

         1 and 7.  The treated  plant demonstrated a  significant

         increase in the root growth, as well as in the number of

         nodules present.

 

                EXAMPLE 9

 

         A laboratory test was conducted comparing germination of

         hybrid seed  corn  coated with  the  fertilizer  of  the

         present invention  at varying  levels of  active  agent.

         The corn was allowed to germinate in filter paper,  kept

         moist with sterilized  distilled water.   The  test  was

         conducted with  plain corn  and with  corn treated  with

         Aspergillus flavus,oryzae  active agent  at 20  ppm,  25

         ppm, and 30 ppm in  sand washings.   After two weeks  of

         growth, the seedlings  were mounted on  graph paper  and

         allowed to dry.  Measurements were taken of the root and

         stalk growth for ten  seedlings  for each  group.    The

         results are  shown  below.    The  measurements  are  in

         centimeters +0.4 centimeters.

 

                 Control     20 ppm       25 ppm        30 ppm

              Stalk/Root   Stalk/Root   Stalk/Root   Stalk/Root  

     Kernel         Growth       Growth       Growth       Growth

    1       4.8/1.8        5.0/1.2       5.0/13.2   5.0/5.6

    2       4.4/2.0        4.6/6.4       5.8/6.4     4.6/2.4

    3       4.6/0.2        4.2/8.6       5.4/7.0     3.6/2.0      

    4       3.6/3.8        3.6/2.0       5.6/3.0     2.0/3.4       

    5       2.8/3.4        3.2/6.0       5.2/8.4     4.2/4.8

    6       2.2/0.2        3.4/4.0       4.4/8.0     3.2/2.4         

    7       2.2/0.4        3.0/5.6       4.5/9.4     3.2/4.2

    8       2.8/3.0        2.4/2.0       4.0/7.4     2.5/0  

    9       ------            1.6/0         4.0/7.4     1.2/1.8

    10      ------           1.2/2.3       2.4/6.4     1.5/2.8


                    

                                                 

         The increase in root  and stalk growth  for the  treated

         seeds was striking.   The  test  demonstrates  that  the

         optimal level of active agent was 25 ppm.  The foregoing

         example Show that the fertilizer in accordance with  the

         invention is an  effective fertilizer  and plant  growth

         and yield promoter.  Although  the preferred  embodiment

         of this  invention  has been  shown  and  described,  it

         should be understood that  various modifications may  be

         reverted to without  departing  from the  scope  of  the

         invention as disclosed and claimed herein.

 

        What is claimed is:

         1.  A fertilizer  which produces increased  yields of  a

         food crop  producing plant,  which comprises  less  than

         1.05% of an active agent  consisting of a fungus of  the

         species Aspergillus Flavus Oryzae which can be grown  at

         temperatures up to 30' C.  and possesses the ability  to

         fix nitrogen and  to  incorporate it  into  chitin,  the

         active agent being substantially uniformly dispersed  in

         a carrier that is stable during storage and non-toxic to

         the plant wherein the carrier is  chosen from the  group

         consisting of  finely ground  calcium  carbonate,  talc,

         sand, sand washings,  and  silt.    2.    A  method  for

         increasing the yield of a food crop yielding plant which

         comprises treating the food crop yielding plant with  an

         effective amount of fertilizer to  cause an increase  in

         the food crop yield, the fertilizer comprising less than

         0.05% of an active agent  consisting of a fungus of  the

         species Aspergillus Flavus Oryzae which can be grown  at

         temperatures up to 30 degrees C.  and posses the ability

         to fix nitrogen and to incorporate  it into chitin,  the

         active agent being substantially uniformly dispersed  in

         a carrier that is stable during storage and non-toxic to

         the plant 3.   A  method  in accordance  with  claim  2,

         wherein the plant is  grown from seed,  and the seed  is

         coated with the fertilizer.  4.  A method in  accordance

         with claim 2, wherein the plant is grown from a  cutting

         having a cut  end and  the  cut end  of the  cutting  is

         dusted with the fertilizer.  5.  A method in  accordance

         with claim 2, wherein the plant is grown from a seedling

         having roots, and the fertilizer is dusted on the  roots

         of the seedling.  6.  A method for increasing the  yield

         of a food crop yielding  plant which comprises  treating

         the soil in which the food crop yielding plant is  grown

         with a fertilizer, the  fertilizer comprising less  than

         0.5% of an active  agent consisting of  a fungus of  the

         species Aspergillus Flavus oryzae which can be grown  at

         temperatures up to 30 degrees C.  and posses he  ability

         to fix nitrogen and to incorporate  it into chitin,  the

         active agent being substantially uniformly dispersed  in

         a carrier that is stable during storage and non-toxic to

         the plant.